HCID 12080904、化合物 → 5-Ethynylisophthalic acid
反応式
[C:1]([C:3]1[CH:4]=[C:5]([C:12]([O-:14])=[O:13])[CH:6]=[C:7]([CH:11]=1)[C:8]([O-:10])=[O:9])#[CH:2].[K+].[K+]>O>[C:1]([C:3]1[CH:4]=[C:5]([C:12]([OH:14])=[O:13])[CH:6]=[C:7]([CH:11]=1)[C:8]([OH:10])=[O:9])#[CH:2]参加物
3
実験手順
Dipotassium 5-ethynylisophthalate in an amount of 5 g (0.019 moles) was dissolved into 20 ml of ion-exchanged water and insoluble substances were removed by filtration with a 5C filter paper. To the obtained filtrate, a 5 moles/liter hydrochloric acid was added under stirring until the pH became 1. The formed solid substance was separated by filtration, washed with ion-exchanged water and filtered. The filtration and the washing were repeated twice. The obtained solid substance was dried at 50° C. under a reduced pressure and 3.6 g of 5-ethynylisophthalic acid was obtained (the yield: 99.5%).
後処理
- customwere removed by filtration with a 5C
- filtrationfilter paper
- additionTo the obtained filtrate, a 5 moles/liter hydrochloric acid was added
- customThe formed solid substance was separated by filtration
- washwashed with ion-exchanged water
- filtrationfiltered
- filtrationThe filtration
- customThe obtained solid substance was dried at 50° C. under a reduced pressure
出典と根拠
- ORDレコード
- ord-07eaffbab5934c26998901ecd7cf5333
- 出典データセット
- uspto-grants-2005_09
- 特許番号
- US06949674B2
反応ノート
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