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3-(Imidazol-5-yl)-5-methoxy-6-methylindene → HCID 67529444、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Imidazol-5-yl)-5-methoxy-6-methylindene | HCID 67530783 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 触媒 | Platinum oxide monohydrate | HCID 86587499 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 67529444 | HCID 67529444 | — |
反応手順
This compound was prepared in a manner analogous to that of Step E of Example 1, by the hydrogenation of 0.5 gram (0.0022 mole) of 3-(imidazol-5-yl)-5-methoxy-6-methylindene (viii) in the presence of 0.1 gram (catalyst) of 10% palladium on carbon and 0.1 gram (catalyst) of platinum oxide hydrate in 40 mL of ethanol. The yield of subject compound was 0.42 gram, mp 68-70° C. The NMR spectrum was consistent with the proposed structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07767667B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-ddef700dccce4e6487c6d9dacbbe1683 |
| 出典メモ | uspto-grants-2010_08 |