Hydrochloric Acid → 2-Aminoquinoline-6-carboxylic Acid Hydrochloride
反応式
[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([O:14]CC)=[O:13])[CH:8]=2)[N:3]=1.[ClH:17]>>[ClH:17].[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([C:12]([OH:14])=[O:13])[CH:8]=2)[N:3]=1参加物
3
実験手順
330 mg of ethyl 2-aminoquinoline-6-carboxylate was stirred in 30 ml of 6 M hydrochloric acid at 80° C. overnight. The solvent was evaporated, and the residue was washed with ethyl acetate to obtain the title compound.
後処理
- customThe solvent was evaporated
- washthe residue was washed with ethyl acetate
出典と根拠
- ORDレコード
- ord-433f363192db47b18bcac0f46394763f
- 出典データセット
- uspto-grants-2004_03
- 特許番号
- US06710056B2
反応ノート
読み込み中…