関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 1,4-Dioxane | HCID 31275 | — |
| 反応物 | 5-Nitro-2-thenoic acid | HCID 80591 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Ethyl 5-nitrothiophene-2-carboxylate | HCID 304627 | — |
反応手順
5 g of 5-nitrothiophene-2-carboxylic acid was stirred in 100 ml of ethanol. 20 ml of dioxane containing 4 M of hydrogen chloride was added to the obtained mixture, and they were stirred at 60° C. for 2 days. The solvent was evaporated to obtain the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06710056B2 |
|---|
| 出典データセット | uspto-grants-2004_03 |
|---|
| ORD ID | ord-f84d5a426a894c01af94fb8ebc136096 |
|---|
| 出典メモ | uspto-grants-2004_03 |
|---|
