関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Cyanamide | HCID 9864 | — |
| 反応物 | 4-(Aminomethyl)Benzoic Acid | HCID 65526 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178512765 | HCID 178512765 | — |
反応手順
A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06710056B2 |
|---|
| 出典データセット | uspto-grants-2004_03 |
|---|
| ORD ID | ord-c887df8de4df4a55a09c1569fe4de64f |
|---|
| 出典メモ | uspto-grants-2004_03 |
|---|
