化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Dimethylisoxazole-4-isocyanate → 1-(3,5-Dimethylisoxazol-4-yl)carbamoylcyclopropanesulfonamide tert-butylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dimethylisoxazole-4-isocyanate | HCID 2736266 | — |
| 反応物 | 1-Methoxymethylcyclopropylsulfonylamine tert-butylcarbamate | HCID 66752382 | — |
| 生成物 | 1-(3,5-Dimethylisoxazol-4-yl)carbamoylcyclopropanesulfonamide tert-butylcarbamate | HCID 66752480 | 100% |
反応手順
This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butylcarbamate except that 1.20 equivalents of 3,5-dimethylisoxazole-4-isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07772180B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-ff598d96d2ea4b16b39088dd92608f84 |
| 出典メモ | uspto-grants-2010_08 |