化工社化工社 化学情報印刷レポート · 研究参考用
Toluene → Dicyclopentadiene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Cyclopentadiene | HCID 7612 | — |
| 反応物 | Acrylate | HCID 25188 | — |
| 生成物 | Dicyclopentadiene | HCID 6492 | — |
反応手順
The derivative was synthesized as follows. 20 grams of the derivative of acrylate obtained as the third example was dissolved in 20 milliliters of toluene. 7 grams of cyclopentadiene was dropped into the solution cooled with ice, and was agitated through all night. Dicyclopentadiene was produced as by-product, and was eliminated in vacuum. Then, 24.9 grams of the derivative of norbornene was obtained. The derivative of norbornene was viscous liquid, and the yield was 95%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06710188B2 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-ed221a40b0554bbd900e864b34ebf7eb |
| 出典メモ | uspto-grants-2004_03 |