4-Pyridinecarboxaldehyde → HCID 136059627、化合物
反応式
[NH2:1][C:2]1[C:3](=[O:10])[N:4]([CH3:9])[N:5]=[CH:6][C:7]=1[NH2:8].[N:11]1[CH:16]=[CH:15][C:14]([CH:17]=O)=[CH:13][CH:12]=1>[N+](C1C=CC=CC=1)([O-])=O>[CH3:9][N:4]1[C:3](=[O:10])[C:2]2[N:1]=[C:17]([C:14]3[CH:15]=[CH:16][N:11]=[CH:12][CH:13]=3)[NH:8][C:7]=2[CH:6]=[N:5]1参加物
4
反応条件
- 温度
- 190 °C
実験手順
0.560 g of 4,5-diamino-2-methyl-2H-pyridazin-3-one and 0.535 g of 4-pyridinecarbaldehyde were added to 10 ml of nitrobenzene, and the mixture was heated at 190° C. under a nitrogen atmosphere for three hours. The reaction solution was cooled down, and the precipitate was collected by filtration to give 0.381 g of the title compound.
後処理
- temperatureThe reaction solution was cooled down
- filtrationthe precipitate was collected by filtration
出典と根拠
- ORDレコード
- ord-4d8f31411cdd4040a7147e2c401d4e14
- 出典データセット
- uspto-grants-2010_08
- 特許番号
- US07772226B2
反応ノート
読み込み中…