Hydrochloric Acid → Ethyl 2-(4-(bromomethyl)phenyl)acetate
反応式
[Br:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([OH:12])=[O:11])=[CH:5][CH:4]=1.Cl.[CH2:14](O)[CH3:15]>>[Br:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][C:10]([O:12][CH2:14][CH3:15])=[O:11])=[CH:7][CH:8]=1参加物
4
実験手順
1.00 g of 2-[4-(bromomethyl)phenyl]acetic acid was suspended in 5 mL of a 4M solution of hydrogen chloride in ethanol, and this suspension was stirred for 2 hours at room temperature. The reaction mixture was concentrated under reduced pressure to yield 0.954 g of ethyl 2-[4-(bromomethyl)phenyl]acetate as light brown oil.
後処理
- concentrationThe reaction mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-119996c9d6a74b3a81f1179dd077e064
- 出典データセット
- uspto-grants-2010_08
- 特許番号
- US07772285B2
反応ノート
読み込み中…