化工社化工社 化学情報印刷レポート · 研究参考用
Sodium hydride → 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | 2-Thienylacetonitrile | HCID 72880 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile | HCID 65353080 | — |
反応手順
Thiophene-2-acetonitrile and 1,4-dichloride-2-butene were added to a DMF solution of sodium hydride washed with hexane and the whole was reacted at room temperature to obtain 1-(2-thienyl)cyclopent-3-ene-1-carbonitrile.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07776897B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-8008992ec5f640278445eefa7cfdca24 |
| 出典メモ | uspto-grants-2010_08 |