化工社化工社 化学情報印刷レポート · 研究参考用
Methanol--water (1/1) → 1,17-Biscyclohexylguanidino-9-azaheptadecane triacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol--water (1/1) | HCID 22242641 | — |
| 反応物 | 1,17-Biscyclohexylguanidino-9-azaheptadecane dihydroiodide | HCID 131718108 | — |
| 生成物 | 1,17-Biscyclohexylguanidino-9-azaheptadecane triacetate | HCID 131718106 | — |
反応手順
10.2 g (0.011 mol) of 1,17-biscyclohexylguanidino-9-azaheptadecane dihydroiodide in 150 ml of methanol/water (1:1) were filtered through a column containing 250 g of ion exchanger (OH- form). The free guanidine base obtained after working up was dissolved in methanol and converted into the triacetate with excess glacial acetic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05242948 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-4bb73f6b08114a6bb1231cd70986f4d3 |
| 出典メモ | uspto-grants-1993_09 |