化工社化工社 化学情報印刷レポート · 研究参考用
4-Bromostyrene → 4,4'-Dibromostilbene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Bromostyrene | HCID 16263 | — |
| 触媒 | HCID 178479819 | HCID 178479819 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 4,4'-Dibromostilbene | HCID 53395981 | — |
反応手順
To a three neck 50 ml round bottom, 4-bromostyrene (14.490 g, 0.0786 mol) was added. To the solution, a magnetic stir bar along with dichloromethane (DCM) (10 mL) were added. To the solution, Grubb's catalyst (0.500 mg, 5.8×10−4 mol) along with DCM (25 mL) was added. The solution was allowed to react for 24 hours at room temperature. The precipitate was filtered and placed into a vial for storage.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07777176B2 |
| 出典データセット | uspto-grants-2010_08 |
| ORD ID | ord-7f80ae51b39a49fdba2b869075d15d29 |
| 出典メモ | uspto-grants-2010_08 |