2-Methylbenzoic acid → 2-Methyl-N-(1-methyl-4-phenyl-piperidin-4-ylmethyl)-benzamide
反応式
[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:11][N:12]1[CH2:17][CH2:16][C:15]([CH2:24][NH2:25])([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:14][CH2:13]1>>[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:25][CH2:24][C:15]1([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:14][CH2:13][N:12]([CH3:11])[CH2:17][CH2:16]1)=[O:6]参加物
3
実験手順
From 2-methylbenzoic acid and C-(1-methyl-4-phenyl-piperidin-4-yl)-methylamine. LCMS (MH+): m/z=323.1, tR (minutes, Method A)=0.56
出典と根拠
- ORDレコード
- ord-10ef5e8622ed4394a833d5b2d8f90073
- 出典データセット
- uspto-grants-2015_08
- 特許番号
- US09102591B2
反応ノート
読み込み中…