Water → Water Formic Acid Benzyl Formate

HRID 51239

反応式

HRID 51239 の反応式
O.[CH:2]([O:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=[O:3]>C(O)=O>[OH2:3].[CH:2]([OH:4])=[O:3].[CH:2]([O:4][CH2:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)=[O:3]

参加物

4

反応物 2

HCID 962WaterHCID 7708Benzyl formate

生成物 1

HCID 86759410Water Formic Acid Benzyl Formate

試薬・触媒・溶媒 1

HCID 284Formic Acid溶媒

実験手順

A mixture of water (10.0061 g) and benzyl formate (E, 10.7949 g) was in each case introduced into a thermostated glass vessel and stirred at 20.0 (±0.2)° C. In each case, a small amount of formic acid was added to this mixture. After vigorous mixing, the stirrer was stopped and phase separation was awaited. Samples were in each case taken from the water phase and the benzyl formate phase and their formic acid content analyzed. The values determined are given in Table 5.

後処理

  1. additionintroduced into a thermostated glass vessel
  2. customphase separation

出典と根拠

ORDレコード
ord-465234f8f8cf490d9ea5db03125392bd
出典データセット
uspto-grants-2004_03
特許番号
US06713649B1

関連ノート

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