化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Octyl acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Acrylic Acid | HCID 6581 | — |
| 反応物 | 1-Octene | HCID 8125 | — |
| 生成物 | Octyl acrylate | HCID 17258 | — |
反応手順
To 1.00 g (0.00891 mole, 1 eq) of 1-octene heated to 50° C. was added a solution of 0.706 g (0.00980 mole, 1.1 eq) of acrylic acid and 2.00 g of a 96 wt-% solution of sulfuric acid (18 M, 0.0196 mole, 2.2 eq). After 15 minutes at 70° C. all the olefin was consumed but only 30% of the product was the desired acrylate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09102774B2 |
| 出典データセット | uspto-grants-2015_08 |
| ORD ID | ord-12243f2f6dd04e45a83cbcd11720b0b6 |
| 出典メモ | uspto-grants-2015_08 |