化工社化工社 化学情報印刷レポート · 研究参考用
Dihydrocoumarin → 4-Hydroxy-1-indanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dihydrocoumarin | HCID 660 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 生成物 | 4-Hydroxy-1-indanone | HCID 590547 | — |
反応手順
4-Hydroxy-1-indanone (76) was synthesized by aluminum chloride induced re-cyclization of dihydrocumarin (75), according to Org. Lett., 2007, 9(15), p. 2915-2918. The reaction was performed on 100 g of (75) to furnish (76) with 85% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09108916B2 |
| 出典データセット | uspto-grants-2015_08 |
| ORD ID | ord-07f7d30e0d48480a86a96aa16b53371a |
| 出典メモ | uspto-grants-2015_08 |