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(4-Bromophenoxy)(tert-butyl)dimethylsilane → 5-[(4-{[tert-Butyl(dimethyl)silyl]oxy}phenyl)amino]-1-methyl-1H-pyrazole-3-carbonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-Bromophenoxy)(tert-butyl)dimethylsilane | HCID 4227167 | — |
| 反応物 | 4-((Tert-butyldimethylsilyl)oxy)aniline | HCID 11715553 | — |
| 反応物 | 5-Amino-1-methyl-1H-pyrazole-3-carbonitrile | HCID 57893830 | — |
| 生成物 | 5-[(4-{[tert-Butyl(dimethyl)silyl]oxy}phenyl)amino]-1-methyl-1H-pyrazole-3-carbonitrile | HCID 131733319 | — |
反応手順
The procedure is in accordance with the protocol of Step B of Preparation 1″, replacing the 4-bromo-1-methyl-1H-pyrazole by (4-bromophenoxy)-(tert-butyl)dimethyl-silane and the 4-{[tert-butyl(dimethyl)silyl]oxy}aniline by the compound from Step A.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09108983B2 |
| 出典データセット | uspto-grants-2015_08 |
| ORD ID | ord-3b6f9154a7f64d0d93eb1c157918f538 |
| 出典メモ | uspto-grants-2015_08 |