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HRID 516272作成日:2026年10月26日

(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal → Levoglucosan

https://huagongshe.com/reaction/516272

反応式

関与物質

役割名称HCID仕込み量
反応物(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanalHCID 107526—
溶媒Sulfuric AcidHCID 1118—
生成物LevoglucosanHCID 2724705—

反応条件

温度90 °C

反応手順

Prior to the glucose determination, the maltodextrins and the various copolymers were hydrolysed following the following sulfuric acid procedure. About 500 mg sample was weighed in an acid digestion bomb equipped with 30 ml teflon insert (Parr Instruments) and diluted with 1 ml 70% H2SO4 followed by addition of approximately 3 ml of distilled (milliQ) water. The mixture was heated to 90° C. for about 5 hours. This hydrolysis was carried out in duplicate for all samples.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09109068B2
出典データセットuspto-grants-2015_08
ORD IDord-bc9d456af2124ba1b3af295ed003b110
出典メモuspto-grants-2015_08