関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| 溶媒 | Sulfuric Acid | HCID 1118 | — |
| 生成物 | Levoglucosan | HCID 2724705 | — |
反応手順
Prior to the glucose determination, the maltodextrins and the various copolymers were hydrolysed following the following sulfuric acid procedure. About 500 mg sample was weighed in an acid digestion bomb equipped with 30 ml teflon insert (Parr Instruments) and diluted with 1 ml 70% H2SO4 followed by addition of approximately 3 ml of distilled (milliQ) water. The mixture was heated to 90° C. for about 5 hours. This hydrolysis was carried out in duplicate for all samples.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US09109068B2 |
|---|
| 出典データセット | uspto-grants-2015_08 |
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| ORD ID | ord-bc9d456af2124ba1b3af295ed003b110 |
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| 出典メモ | uspto-grants-2015_08 |
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