関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methacrylic anhydride | HCID 12974 | — |
| 反応物 | 2-(N-ethylanilino)ethanol | HCID 62338 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 2-[Ethyl(phenyl)amino]ethyl prop-2-enoate | HCID 19097126 | — |
反応手順
Methacrylic anhydride (7.7 g, 0.05 mol) is added to a solution of N-(2-hydroxyethyl)-N-ethylaniline (6.6 g, 0.04 mol) in pyridine (25 ml) and the mixture is stirred at 55° C. for 2 hours. On cooling the mixture is passed through silica gel to give N-(2-acryloyloxyethyl)-N-ethylaniline as a pale yellow oil. 5.3 g, 65%
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09115464B2 |
|---|
| 出典データセット | uspto-grants-2015_08 |
|---|
| ORD ID | ord-b6a855aa18e948d3a1b8c85244d381bf |
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| 出典メモ | uspto-grants-2015_08 |
|---|
