反応式
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][C:7](Cl)=[O:8].[NH4+:10].[OH-]>>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][C:7]([NH2:10])=[O:8]参加物
3
実験手順
To a mixture of concentrated NH4OH (100 mL) and ice was added 2-thiopheneacetyl chloride (13.0 g, 80.9 mmol). The desired compound crystallized from the reaction mixture. Recrystallization from hot water gave 2-thiopheneacetamide (8.08 g, 64% yield) as white crystals. mp 146°-147° C.
後処理
- customThe desired compound crystallized from the reaction mixture
- customRecrystallization from hot water
出典と根拠
- ORDレコード
- ord-d50cdad937b642df885f4e3877aa82ac
- 出典データセット
- uspto-grants-1997_04
- 特許番号
- US05616596
関連ノート
読み込み中…