関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Propylhept-2-enal | HCID 118745 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 生成物 | 2-Propylheptanal | HCID 3018634 | 97.8% |
反応手順
An autoclave was charged with 420 g of 2-propyl-2-heptenal and 4 g of a 5% Pd carbon powder (water content: 56%, manufactured by N.E. Chemcat Corporation), and the mixture was stirred at 75° C. for 1.5 hours under a hydrogen pressure of 1.5 MPa. The reaction product was filtered through a membrane filter (PTFE, 0.5 μm) to obtain 416 g of 2-propylheptanal.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09328306B2 |
|---|
| 出典データセット | uspto-grants-2016_05 |
|---|
| ORD ID | ord-f577967a37614483969cbe2e27e6788d |
|---|
| 出典メモ | uspto-grants-2016_05 |
|---|
