化工社化工社 化学情報印刷レポート · 研究参考用
Heptanoic Acid → 2-Propylheptanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Heptanoic Acid | HCID 8094 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-Propylheptanal | HCID 3018634 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-Propylheptanoic acid | HCID 35728 | — |
反応手順
A reactor was charged with 0.2 g (0.005 mol) of sodium hydroxide (manufactured by Kanto Chemical Co., Inc.), 1 g of water, and 0.8 g (0.006 mol) of heptanoic acid (manufactured by Kishida Chemical Co., Ltd.), and the mixture was stirred. After the addition of 47 g of 2-propylheptanal, the mixture was bubbled with air at 40° C. for 15 hours. The mixture was stirred at 130° C. for 4 hours with nitrogen bubbling to obtain crude 2-propylheptanoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09328306B2 |
| 出典データセット | uspto-grants-2016_05 |
| ORD ID | ord-60a94c02c1db45ad99ce7e0235de28e4 |
| 出典メモ | uspto-grants-2016_05 |