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Potassium Carbonate → S 20928
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| 反応物 | 2-(1-Naphthyl)ethylamine hydrochloride | HCID 12370437 | — |
| 溶媒 | Chloroform water | HCID 22418719 | — |
| 生成物 | S 20928 | HCID 127856 | — |
反応手順
0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05616614 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-8e4b4b7fd8854a2684e0c0c78407b175 |
| 出典メモ | uspto-grants-1997_04 |