Ammonia → Morpholine-3-carboxamide

HRID 524588

反応式

HRID 524588 の反応式
Cl.[NH:2]1[CH2:7][CH2:6][O:5][CH2:4][CH:3]1[C:8]([O:10]C)=O.[NH3:12]>CO>[NH:2]1[CH2:7][CH2:6][O:5][CH2:4][CH:3]1[C:8]([NH2:12])=[O:10]

参加物

4

反応物 2

HCID 222AmmoniaHCID 42614243Methyl morpholine-3-carboxylate--hydrogen chloride (1/1)

生成物 1

HCID 19792002Morpholine-3-carboxamide収率 99%

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

A mixture of methyl morpholine-3-carboxylate hydrochloride (0.55 g, 3.0 mmol) and a solution of NH3 in methanol (7 mol/L, 20 mL) was stirred at 50° C. for 24 hours in a sealed tube. The mixture was concentrated in vacuo to give the title compound as glutinous semisolid (0.39 g, 99%). The compound was characterized by the following spectroscopic data:

後処理

  1. concentrationThe mixture was concentrated in vacuo

出典と根拠

ORDレコード
ord-13e5a44e7f7c4fccb815db4929082891
出典データセット
uspto-grants-2016_05
特許番号
US09340538B2

関連ノート

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