化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-6-methoxybenzothiazole → 2-Cyano-6-methoxy benzothiazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-6-methoxybenzothiazole | HCID 15630 | — |
| 反応物 | HCID 178418546 | HCID 178418546 | — |
| 生成物 | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | 22.1% |
反応手順
6-methoxybenzo[d]thiazol-2-amine (9 g, 50 mmol) was reacted with CuCN (8.96 g, 100 mmol) according to the procedure as described in Example 61, Step A to give the title compound as a white solid (2.1 g, 22%). The compound was characterized by the following spectroscopic data:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09340538B2 |
| 出典データセット | uspto-grants-2016_05 |
| ORD ID | ord-f2c31f5651ce4d4bbb0f55cdedf1b63b |
| 出典メモ | uspto-grants-2016_05 |