5-Methoxy-1,3-thiazol-2-amine → 5-Methoxythiazole-2-carbonitrile
反応式
[CH3:1][O:2][C:3]1[S:7][C:6](N)=[N:5][CH:4]=1.[C:9]([Cu])#[N:10]>>[CH3:1][O:2][C:3]1[S:7][C:6]([C:9]#[N:10])=[N:5][CH:4]=1参加物
3
実験手順
5-methoxythiazol-2-amine (2.6 g, 20 mmol) was reacted with CuCN (4 g, 44 mmol) according to the procedure as described in Example 61, Step A to give the title compound as brownish oil (0.84 g, 30%). The compound was characterized by the following spectroscopic data:
出典と根拠
- ORDレコード
- ord-b60f1450e100498aa2dcb7364c0119c2
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09340538B2
反応ノート
読み込み中…