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HRID 52587作成日：2026年10月26日
Acetic Anhydride → (R)-N2-Acetyl-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide
https://huagongshe.com/reaction/52587
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 反応物 | (R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamide | HCID 136381090 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | (R)-N2-Acetyl-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide | HCID 136381103 | — |
反応手順
0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino) methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05616620 |
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| 出典データセット | uspto-grants-1997_04 |
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| ORD ID | ord-32448bb5a54f41b6969b78bc6789bb71 |
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| 出典メモ | uspto-grants-1997_04 |
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