化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Civetone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Ethyl 17-oxocycloheptadec-8-ene-1-carboxylate | HCID 53673108 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Civetone | HCID 5315941 | — |
反応手順
2-ethoxycarbonyl-9-cycloheptadecenone will be refluxed with about 10% NaOH in methanol for about 1 hour to give civetone. After completion of the reaction, the reaction mixture will be neutralized using about 10% sulfuric acid. The product will be extracted using ether and can be purified using silica-gel chromatography.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09346729B2 |
| 出典データセット | uspto-grants-2016_05 |
| ORD ID | ord-00fc4ff0450f49bc9168967cb6cbe090 |
| 出典メモ | uspto-grants-2016_05 |