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Triethoxysilane → Triethoxy(3-isocyanatopropyl)silane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethoxysilane | HCID 13830 | — |
| 反応物 | Allyl isocyanate | HCID 15123 | — |
| 溶媒 | P-Xylene | HCID 7809 | — |
| 生成物 | Triethoxy(3-isocyanatopropyl)silane | HCID 90613 | 71.8% |
反応手順
In analogy to Example 6, a reaction mixture consisting of 640 g of p-xylene, 680 g (8.17 mol) of allyl isocyanate and 1250 g (7.6 mol) of triethoxysilane was reacted at from 76° to 92° C. over the course of 150 minutes. Working up by distillation gave 1350 g of 3-isocyanatopropyltriethoxysilane in addition to the trimer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05616762 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-a6b7d28bd66448d9ab588797d7716d9f |
| 出典メモ | uspto-grants-1997_04 |