化工社化工社 化学情報印刷レポート · 研究参考用
1-Phenethylamine, (-)- → 1-Phenethylamine, (-)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Phenethylamine, (-)- | HCID 75818 | — |
| 反応物 | 3-(Carbamoylmethyl)-5-methylhexanoic acid | HCID 10867083 | — |
| 生成物 | 1-Phenethylamine, (-)- | HCID 75818 | — |
| 生成物 | (3S)-3-(2-Amino-2-oxoethyl)-5-methylhexanoic acid | HCID 22871591 | — |
反応手順
Combining (±)-3-(carbamoylmethyl)-5-methylhexanoic acid with (S)-(-)-α-phenylethylamine in a solution to obtain the (S)-(-)-α-phenylethylamine salt of (S)-(+)-3-(carbamoylmethyl)-5-methylhexanoic acid, which crystallizes out of the solution;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05616793 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-4e4694c3e4b3494fa0872831e08c4df8 |
| 出典メモ | uspto-grants-1997_04 |