Hydrochloric Acid → Hydrochloric Acid
反応式
C(OC([N:8]1[CH2:11][CH:10]([C:12]2[O:13][C:14]([CH3:17])=[CH:15][N:16]=2)[CH2:9]1)=O)(C)(C)C.[ClH:18]>O1CCOCC1>[ClH:18].[NH:8]1[CH2:11][CH:10]([C:12]2[O:13][C:14]([CH3:17])=[CH:15][N:16]=2)[CH2:9]1.[ClH:18]参加物
5
実験手順
To 57 mg (0.24 mmol) 3-(5-methyl-oxazol-2-yl)-azetidine-1-carboxylic acid tert-butyl ester was added 2 mL (8 mmol) HCl in dioxane (4 M), and the reaction was stirred at room temperature for 1 hour. The solvent was evaporated to give the desired product as a HCl salt, which was used for the next step without further purification.
後処理
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-0f29d1d5d926482f8b6efb58f7f58d2c
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09346816B2
反応ノート
読み込み中…