Benzylamine → HCID 118201132、化合物
反応式
[CH2:1]([NH2:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:9]1([CH2:13][CH:14]=O)[CH2:12][CH2:11][CH2:10]1>C(Cl)Cl>[CH:9]1([CH2:13][CH:14]=[N:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH2:12][CH2:11][CH2:10]1参加物
4
実験手順
Benzylamine (2.95 g, 27.5 mmol) was added to a mixture of cyclobutylacetaldehyde (30.6 mmol) in CH2Cl2 (˜238 mL) and molecular sieves (5.0 g) and the mixture was stirred at room temperature for 5.5 hours. The mixture was filtered over Celite and the solvent was removed under vacuum to yield 5.45 g of crude N-(2-cyclobutylethylidene)-1-phenylmethanamine.
後処理
- filtrationThe mixture was filtered over Celite
- customthe solvent was removed under vacuum
出典と根拠
- ORDレコード
- ord-68fd615743254ce5821775dd2ee41d1b
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09346853B2
反応ノート
読み込み中…