化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexanone → 1-Hydroxycyclohexyl phenyl ketone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexanone | HCID 7967 | — |
| 反応物 | epsilon-CAPROLACTONE | HCID 10401 | — |
| 反応物 | Acrylate | HCID 25188 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | 1-Hydroxycyclohexyl phenyl ketone | HCID 70355 | — |
反応手順
To 900 parts by weight of methyl ethyl ketone were added 100 parts by weight of cyclohexanone, 750 parts by weight of partially caprolactone-modified polyfunctional acrylate (DPCA-20, produced by Nippon Kayaku Co., Ltd.), 200 parts by weight of a silica sol (MIBK-ST, produced by Nissan Chemical Industries, Ltd.) and 50 parts by weight of a photopolymerization initiator (IRGACURE 184, produced by Ciba Specialty Chemicals Corp.), followed by stirring. The mixture was filtered through a polypropylene filter having a pore size of 0.4 μm to prepare Coating solution A for hardcoat layer.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09346961B2 |
| 出典データセット | uspto-grants-2016_05 |
| ORD ID | ord-9a57fa932ad648018dd025c593e3007b |
| 出典メモ | uspto-grants-2016_05 |