関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 4-Pentenoic acid, phenylmethyl ester | HCID 10052035 | — |
| 反応物 | 1-Chlorosilolane | HCID 71364168 | — |
| 生成物 | HCID 90417926 | HCID 90417926 | — |
反応手順
To a mixture of crude 1-chlorosilolane (0.317 g) and benzyl pent-4-enoate (0.50 g; 2.63 mmol) under argon was added two drops of Karstedt's catalyst solution (in xylenes; ˜2% Pt). The reaction vessel was sealed and the mixture was heated to 60° C. for 18 hours. The crude liquid was used without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09352049B2 |
|---|
| 出典データセット | uspto-grants-2016_05 |
|---|
| ORD ID | ord-822de5eb39cf41d8a61145a148ccab26 |
|---|
| 出典メモ | uspto-grants-2016_05 |
|---|
