2-propyl-1H-imidazole-4,5-dicarbonitrile → HCID 178450364、化合物
反応式
[C:1]([C:4]1[N:5]=[C:6]([CH2:11][CH2:12][CH2:13]C)[NH:7][C:8]=1[C:9]#[N:10])(=[O:3])[CH3:2].[CH2:15](C1NC(C#N)=C(C#N)N=1)[CH2:16]C.C([Mg]Br)CC>>[C:1]([C:4]1[N:5]=[C:6]([CH2:11][CH2:12][CH3:13])[NH:7][C:8]=1[C:9]#[N:10])(=[O:3])[CH2:2][CH2:15][CH3:16]参加物
4
実験手順
Following a procedure similar to that described in Preparation 24(i), but using 2-propylimidazole-4,5-dicarbonitrile (prepared as described in Preparation 10) and propylmagnesium bromide, the title compound, melting at 94°-95° C., was obtained in a 49.8% yield.
出典と根拠
- ORDレコード
- ord-57dbebaf2cb5498081be82cf04d0bd01
- 出典データセット
- uspto-grants-1997_04
- 特許番号
- US05616599
反応ノート
読み込み中…