methyl 1-methyl-1H-pyrazole-3-carboxylate → 1-Methyl-1H-pyrazole-3-carboxamide
反応式
[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]([O:9]C)=O)=[N:3]1.[NH3:11].O>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([C:7]([NH2:11])=[O:9])=[N:3]1参加物
3
実験手順
A solution of methyl 1-methyl-1H-pyrazole-3-carboxylate (1.1 g, 7.9 mmol) in NH3.H2O (10 mL) was stirred for 2 h at room temperature. The solvent was evaporated to give the crude product which was used for the next step without further purification.
後処理
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-c756c510a23a4298a52158dbfa1c4385
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09353104B2
反応ノート
読み込み中…