Azane;hydrate → (3-Ethyl-1-methyl-1H-pyrazol-5-yl)methanamine
反応式
Br[CH2:2][C:3]1[N:7]([CH3:8])[N:6]=[C:5]([CH2:9][CH3:10])[CH:4]=1.[NH3:11].O>>[CH2:9]([C:5]1[CH:4]=[C:3]([CH2:2][NH2:11])[N:7]([CH3:8])[N:6]=1)[CH3:10]参加物
3
実験手順
A solution of compound 5 (660 mg, 3.27 mmol) in NH3.H2O (5 mL) was stirred at 90° C. for 3 h. The solvent was evaporated to give the crude product as a white solid which was used in the next step without further purification.
後処理
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-0c8ed6d935c14741b775cb62fa8cff82
- 出典データセット
- uspto-grants-2016_05
- 特許番号
- US09353104B2
反応ノート
読み込み中…