1,3-Dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene → HCID 71573390、化合物

HRID 532150ノート

反応式

HRID 532150 の反応式
[Cl:1][C:2]1[CH:7]=[C:6]([C:8]([C:10]([F:13])([F:12])[F:11])=[CH2:9])[CH:5]=[C:4]([C:14]([F:17])([F:16])[F:15])[CH:3]=1.ClC1C=C(C(C(F)(F)F)=C)C=C(Cl)C=1.ClC1C=C(C2(C(F)(F)F)[O:44][N:43]=[C:42]([C:45]3[CH:56]=[CH:55][C:48]4[B:49]([OH:54])[O:50][C:51]([CH3:53])([CH3:52])[C:47]=4[CH:46]=3)C2)C=C(Cl)C=1>>[Cl:1][C:2]1[CH:7]=[C:6]([C:8]2([C:10]([F:11])([F:12])[F:13])[O:44][N:43]=[C:42]([C:45]3[CH:56]=[CH:55][C:48]4[B:49]([OH:54])[O:50][C:51]([CH3:53])([CH3:52])[C:47]=4[CH:46]=3)[CH2:9]2)[CH:5]=[C:4]([C:14]([F:15])([F:16])[F:17])[CH:3]=1

参加物

4

反応物 3

HCID 231598231,3-Dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzeneHCID 71573386HCID 71573386、化合物HCID 86654468HCID 86654468、化合物

生成物 1

HCID 71573390HCID 71573390、化合物

実験手順

The title compound was prepared by using the same method as described in 5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)-3,3-dimethyl-benzo[c][1,2]oxaborol-1(3H)-ol with 1-chloro-3-(trifluoromethyl)-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene to replace 1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene. It was obtained as a white solid. MS: m/z=478.1 [M+1]+.

後処理

  1. customIt was obtained as a white solid

出典と根拠

ORDレコード
ord-29f041fd3fd0460b912ddcc2809977c6
出典データセット
uspto-grants-2014_10
特許番号
US08853186B2

反応ノート

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