Oxygen → 1-[3-(3,3-Dimethylbutoxy)-5-ethoxyphenyl]ethanone

HRID 532376

反応式

HRID 532376 の反応式
[OH:1][C:2]1[CH:3]=[C:4]([C:9](=[O:11])[CH3:10])[CH:5]=[C:6]([OH:8])[CH:7]=1.O=O.[CH:14]1(Br)CCCC[CH2:15]1.Br[CH2:22][CH2:23][C:24]([CH3:27])([CH3:26])[CH3:25]>>[CH3:25][C:24]([CH3:27])([CH3:26])[CH2:23][CH2:22][O:1][C:2]1[CH:3]=[C:4]([C:9](=[O:11])[CH3:10])[CH:5]=[C:6]([O:8][CH2:14][CH3:15])[CH:7]=1

参加物

5

実験手順

1-(3,5-Dihydroxyphenyl)ethanone (3.0 g) were converted analogously to O2.031. Instead of cyclohexylbromide, however, 1-bromo-3,3-dimethylbutane was used. After chromatography, 960 mg of the title compound were obtained.

出典と根拠

ORDレコード
ord-eeda2a13305b4368a174816126042f3c
出典データセット
uspto-grants-2014_10
特許番号
US08853206B2

関連ノート

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