Dimethylformamide dimethyl acetal → HCID 68941755、化合物

HRID 532425ノート

反応式

HRID 532425 の反応式
[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:13][CH2:14][C:15]([OH:18])([CH3:17])[CH3:16])=[CH:8][C:9]=1[N+:10]([O-])=O)=[O:4].CO[CH:21]([N:24]([CH3:26])[CH3:25])OC>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([CH2:13][CH2:14][C:15]([OH:18])([CH3:17])[CH3:16])=[CH:8][C:9]=1[N:10]=[CH:21][N:24]([CH3:26])[CH3:25])=[O:4]

参加物

3

反応物 2

HCID 78373Dimethylformamide dimethyl acetalHCID 68936540HCID 68936540、化合物

生成物 1

HCID 68941755HCID 68941755、化合物

実験手順

5-(3-Hydroxy-3-methylbutyl)-3-nitrothiophene-2-carboxylic acid methyl ester was reacted with dimethoxymethyldimethylamine by method B. The product with the molecular weight of 298.41 (C14H22N2O3S) was obtained in this way; MS (ESI): 299.1 (M+H+).

後処理

  1. customThe product with the molecular weight of 298.41 (C14H22N2O3S) was obtained in this way

出典と根拠

ORDレコード
ord-7c8038993ad94062b93c28e50d427627
出典データセット
uspto-grants-2014_10
特許番号
US08853208B2

反応ノート

読み込み中…