化工社化工社 化学情報印刷レポート · 研究参考用
Water → HCID 67316267、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 1-Naphthalenethiol | HCID 68259 | — |
| 反応物 | Ethyl 3-(3-(methylsulfonyloxy)propyl)-1h-indole-2-carboxylate | HCID 87353567 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 67316267 | HCID 67316267 | — |
反応手順
A mixture of EXAMPLE 10A (42 mg), naphthalene thiol (45 mg), and potassium carbonate (36 mg) in acetonitrile (2 mL) was heated at 80° C. for 3 days. The reaction mixture was poured into water, extracted with dichloromethane and purified by flash chromatography on silica gel with 0-20% ethyl acetate in hexanes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08853209B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-e1dfa09626a14fc0925b8340aa0a84fc |
| 出典メモ | uspto-grants-2014_10 |