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Azobenzene → 4-Benzeneazodiphenylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Azobenzene | HCID 2272 | — |
| 溶媒 | Aniline | HCID 6115 | — |
| 生成物 | 4-Benzeneazodiphenylamine | HCID 7575 | 90% |
反応手順
A solution of 25% aqueous tetramethylammonium hydroxide (8 mL) was concentrated under vacuum at 75° C. until solid material formed. Azobenzene (1.8 g) and aniline (10 mL) were added and the solution was stirred under the same conditions for 4 hours and then in the presence of air for 12 hours. Analysis of the reaction by HPLC revealed 90% yield of 4-(phenylazo)diphenylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05618979 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-f005c8cc4f594ec9a2333441f1c54644 |
| 出典メモ | uspto-grants-1997_04 |