化工社化工社 化学情報印刷レポート · 研究参考用
Aniline → N-Cyclohexylaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Nitrobenzene | HCID 7416 | — |
| 反応物 | Cyclohexanone | HCID 7967 | — |
| 反応物 | Diphenylamine | HCID 11487 | — |
| 反応物 | Triphenylamine | HCID 11775 | — |
| 生成物 | N-Cyclohexylaniline | HCID 74567 | 2.9% |
反応手順
Reaction was carried out by the same procedure as in Example I1 except that 32.39 g (0.39 mol) of cyclohexanone, 9.31 g (0.1 mol) of aniline and 24.62 g (0.2 mol) nitrobenzene were used. As a result, the yield of diphenylamine was 89.5%, and 1.8% of triphenylamine and 2.9% of N-cyclohexylaniline were produced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05618980 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-6a4a9d71f6204543b7bc12d011dc8c18 |
| 出典メモ | uspto-grants-1997_04 |