関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-Benzylformamide | HCID 80654 | — |
| 反応物 | Sodium thiocyanate | HCID 516871 | — |
| 生成物 | N-benzyl formamide NaSCN | HCID 131731936 | 100.3% |
反応手順
To a round-bottom flask, 9.9 g of purified N-benzyl formamide and 4 g of NaSCN (sodium thiocyanate) were introduced. The mixture was agitated gradually under nitrogen atmosphere at 30° C. for 40 minutes, and then at room temperature for 5 hours to obtain 10.7 g of N-benzyl formamide-NaSCN eutectic mixture.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08858837B2 |
|---|
| 出典データセット | uspto-grants-2014_10 |
|---|
| ORD ID | ord-92c554d1877b4115a46c924621464c74 |
|---|
| 出典メモ | uspto-grants-2014_10 |
|---|
