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Ethanolamine → Dipyridodiazepinone deriv. 23
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanolamine | HCID 700 | — |
| 反応物 | Dipyridodiazepinone deriv. 15 | HCID 463144 | — |
| 生成物 | Dipyridodiazepinone deriv. 23 | HCID 463150 | — |
反応手順
The title compound, m.p. 241°-244° C., was synthesized from 2-chloro-5,11-dihydro-11-ethyl-4-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and ethanolamine using procedures analogous to those described above, except that the mixture was heated in a pressure bottle at 260° C. for 50 min., and the product was crystallized from chloroform/ethanol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05620974 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-188b5b5854db42b897e43c3abfb0c01f |
| 出典メモ | uspto-grants-1997_04 |