Dimethylamine → 3-chloro-N,N-dimethylpropane-1-sulfonamide
反応式
[Cl:1][CH2:2][CH2:3][CH2:4][S:5](Cl)(=[O:7])=[O:6].[CH3:9][NH:10][CH3:11]>>[Cl:1][CH2:2][CH2:3][CH2:4][S:5]([N:10]([CH3:11])[CH3:9])(=[O:7])=[O:6]参加物
3
実験手順
The procedure used for the preparation of Intermediate D was used to prepare the title compound from 3-chloropropanesulfonyl chloride and dimethylamine. High vacuum drying gave the title compound (2.1 g, 100%): 1H NMR (DMSO-d6) δ: 2.06-2.11 (2H, m), 2.75 (6H, s), 3.10-3.15 (2H, m), 3.72 (2H, t).
出典と根拠
- ORDレコード
- ord-6752174e0ffa469aa497eeb1583e1dba
- 出典データセット
- uspto-grants-2014_10
- 特許番号
- US08859572B2
反応ノート
読み込み中…