2,2-Dimethyl-chroman-4-one → (S)-2,2-dimethylchroman-4-ol

HRID 536457

反応式

HRID 536457 の反応式

[CH3:1][C:2]1([CH3:13])[CH2:11][C:10](=[O:12])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[O:3]1>O.CC#N>[CH3:1][C:2]1([CH3:13])[CH2:11][C@H:10]([OH:12])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[O:3]1

参加物

3

反応物 1

HCID 74542902,2-Dimethyl-chroman-4-one

生成物 1

HCID 11019418(S)-2,2-dimethylchroman-4-ol

試薬・触媒・溶媒 1

HCID 18373917Acetonitrile--water (1/1)溶媒

実験手順

The title compound was prepared from 2,2-dimethylchroman-4-one according to the method described in Example 2B. MS (LCMS) m/z 236 (M+H2O+CH3CN)+.

出典と根拠

ORDレコード: ord-39606b1198c2449b9e712d59938854e4
出典データセット: uspto-grants-2014_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08859584B2

関連ノート

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