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2,4-Dimethoxyphenyl isocyanate → 1-(2,4-Dimethoxyphenyl)-3-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4-Dimethoxyphenyl isocyanate | HCID 601637 | — |
| 反応物 | 4-(4,6-Dimorpholino-1,3,5-triazin-2-yl)aniline | HCID 45379087 | — |
| 生成物 | 1-(2,4-Dimethoxyphenyl)-3-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-urea | HCID 44514202 | — |
反応手順
Starting from 4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)aniline (0.140 g 0.40 mmoles) and 2,4-dimethoxyphenyl isocyanate (131 mg, 0.73 mmoles), the title compound was isolated as a white solid. Yield; 76 mg (36%); (M+H)=522.4
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08859542B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-4e48c6ae3cef467082dcd56c0689dc3d |
| 出典メモ | uspto-grants-2014_10 |