化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dihydroxybutanedioic Acid → cis-Epoxysuccinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dihydroxybutanedioic Acid | HCID 875 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | cis-Epoxysuccinate | HCID 2734802 | — |
反応手順
The resulting heterogeneous reaction mixture, which was lumpy and hardened, was neutralized by addition of 15% aqueous tartaric acid solution. The polymer was filtered and a small portion was ground thoroughly. The ground material was extracted with 2-propanol for 24 hrs in a Soxhlet extractor and dried to afford a pale brown solid which was not soluble to any extent in distilled water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05621088 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-165c21acb8a34d9c9681683a969f54e5 |
| 出典メモ | uspto-grants-1997_04 |