化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl formate → Benzyl [3-(formylamino)propyl]carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl formate | HCID 8025 | — |
| 反応物 | Benzyl (3-aminopropyl)carbamate | HCID 417669 | — |
| 生成物 | Benzyl [3-(formylamino)propyl]carbamate | HCID 86691669 | 99% |
反応手順
Benzyl 3-aminopropylcarbamate 12 (8.00 g, 36.0 mmol) was dissolved in 250 mL of ethyl formate. The solution was refluxed for 4 h. Following complete conversion of the amine, the solution was concentrated to dryness in a rotary evaporator to obtain the formamide as a colorless oil (8.90 g, 99%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08865863B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-e07e3cc5e80d4db8abe3016866640096 |
| 出典メモ | uspto-grants-2014_10 |